Abstract: The subject of this research is the correlation between the policy of neocolonialism and Francophonie in the context of foreign cultural strategy of France in the 1960s. Decolonization forced France to relinquish direct colonial rule and shift towards the policy of “cooperation” on the basis of bilateral agreements with the developing countries, which regulated intergovernmental relations in various spheres. The idea of the universality of French language and cultural values underlied the Agency for Cultural and Technical Cooperation established in 1970. A crucial role in its establishment was played by the political leaders of African countries, who sought benefit from cooperation with France in terms of the development of young sovereign states. Despite this fact, the activity of Francophonie was the object of criticism, and by some researchers, considered a version of French post-colonialism. Analysis is conducted on different interpretations and approaches towards the terms “neo-colonialism” and “Francophonie”. The article employs the unpublished archival documents of the Ministry of Foreign Affairs of France, which determines the scientific novelty. The authors conclude that the equality sign between neo-colonialism and Francophonie seems unreasoned, since the latter has improved the educational, cultural, scientific and technical standard of living in the young sovereign states, contributed to the establishment of their political and administrative and increase of authority on the world stage. The participation of the developing countries in the Agency for Cultural and Technical Cooperation and the leaders of the Western world – France and Canada – consolidated the authority and broadened the experience of the political elite of the third world countries. At the same time, there is no denying that de Gaulle sought to increase the international prestige of the Fifth Republic by strengthening the positions of France in the Francophone world.